HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenyl-2-propyn-1-ol → Benzenepropanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenyl-2-propyn-1-ol | HCID 123115 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzenepropanol | HCID 31234 | 100% |
Reaction Steps
In Example 6, hydrogenation reaction was conducted under the same condition as Example 1 for THF diluted solution concentration of the substance to be reduced, its flow rate, and hydrogen 9 flow rate, using 3-phenyl-2-propin-1-ol as the substance to be reduced. The reaction time was within five minutes. The analytical result of the reaction product by 1H-NMR showed almost complete hydrogenation of 3-phenyl-2-propin-1-ol, and 3-phenyl-1-propanol was obtained at about 100% yield (See FIG. 6.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07663008B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-b3b448576afe4281bec35b958391d547 |
| Source note | uspto-grants-2010_02 |