HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67143095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67141734 | HCID 67141734 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67143095 | HCID 67143095 | 90% |
Reaction Steps
A solution of [7-(3,4-dihydro-1H-isoquinolin-2-yl)-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-5-yl]-(piperidin-1-yl)-methanone prepared in Step 2 in ethyl acetate was saturated with hydrochloric acid gas and then filtered to give the titled compound as a white solid. (Yield: 90%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662832B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-610eb0583e0444a98ab02a2e520224b9 |
| Source note | uspto-grants-2010_02 |