HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86615270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86615268 | HCID 86615268 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86615270 | HCID 86615270 | — |
Reaction Steps
A solution of (1-benzyl-5-chloro-2,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-7-yl)-(4-fluorobenzyl)-carbamic acid tert-butyl ester prepared in Step 3 in ethyl acetate was saturated with hydrochloric acid gas and then filtered. The resulting solid was dried under reduced pressure to give 23.5 mg of the titled compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662832B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-bf8fb293d0e24a8f92be7195497921ef |
| Source note | uspto-grants-2010_02 |