HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86621689, compound → HCID 15985349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86621689 | HCID 86621689 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 15985349 | HCID 15985349 | — |
Reaction Steps
A mixture of 0.020 g [2-((E)-3-{1-[4-(3,5-dimethyl-isoxazol-4-yl)-benzenesulfonyl]-1H-pyrrol-3-yl}-allanoylamino)-phenyl]-carbamic acid tert-butyl ester with a little amount of dioxane and 3 ml 4M HCL in dioxane is stirred at ambient temperature for 1 h. The suspension is centrifuged. The title compound is dried in vacuo. By this method 0.013 g of a red-brown amorph substance are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666868B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-05ecec8696f54e14a69ae6682f19d802 |
| Source note | uspto-grants-2010_02 |