HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 10633517, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethyl 2-amino-2-phenylbutanoate | HCID 10488547 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 10633517 | HCID 10633517 | 100% |
Reaction Steps
12.72 mL of formic acid then 25.38 mL of acetic anhydride were added dropwise, under stirring, to 2.49 g (12.03 mmol) of amine 6. After 15 h at room temperature, solvents were removed under reduced pressure to give 3.09 g of 7 as a green viscous oil (100% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666907B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-2da4ae924bff4504b561554cb1a035c5 |
| Source note | uspto-grants-2010_02 |