HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 24808145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 17beta-Hydroxy wortmannin | HCID 9867340 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 24808145 | HCID 24808145 | — |
Reaction Steps
To a solution of 17-hydroxywortmannin (1100 mg) in methanol (5 mL) is added diethylamine (0.72 mL). After 48 hours the reaction mixture is concentrated under vacuum. The residue is dissolved in EtOAc and precipitated with hexane. A yellow powder is obtained (0.29 mg). MS: 462.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666901B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-6977c54279744414a3cbfd4799c10a7e |
| Source note | uspto-grants-2010_02 |