HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 86598986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Sodium Sulfate | HCID 24436 | — |
| Reactant | Ziprasidone | HCID 60854 | — |
| Reactant | 3-(1-Piperazinyl)-1,2-benzisothiazole monohydrochloride | HCID 11521711 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86598986 | HCID 86598986 | — |
Reaction Steps
In a three necked flask was charged BITP HCl (10 g), CEI (10.35 g) Na2CO3 (14.1 g), Na2SO4 (40 g) and water (50.7 g) and the reaction mixture was heated at reflux for 9 hours. After 9 hours reflux, the ziprasidone peak is 71% area from the reaction mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07667037B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-c3a11c7126244ea09205d3f3f5152f3b |
| Source note | uspto-grants-2010_02 |