HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → 5-(4-Bromophenyl)-N,N-diethylisoxazole-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 5-(4-Bromophenyl)-1,2-oxazole-4-carboxylic acid | HCID 22831701 | — |
| Product | 5-(4-Bromophenyl)-N,N-diethylisoxazole-4-carboxamide | HCID 24809888 | — |
Reaction Steps
The title compound was prepared from 5-(4-bromophenyl)isoxazole-4-carboxylic acid (13.4 mg, 0.050 mmol) and diethylamine (4.4 mg, 0.060 mmol) as described in synthetic method A and thereafter purified by preparative HPLC method A to give a solid (3.8 mg). MS (pos) m/z 323.0 and 325.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-72c35c1673894d37ac73f9f39779cf94 |
| Source note | uspto-grants-2010_02 |