HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → N,N-Diethyl-5-(4-fluorophenyl)isoxazole-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 5-(4-Fluorophenyl)isoxazole-4-carboxylic acid | HCID 3723375 | — |
| Product | N,N-Diethyl-5-(4-fluorophenyl)isoxazole-4-carboxamide | HCID 24809892 | — |
Reaction Steps
The title compound was prepared from 5-(4-fluorophenyl)isoxazole-4-carboxylic acid (10.4 mg, 0.050 mmol) and diethylamine (4.4 mg, 0.060 mmol) as described in synthetic method A and thereafter purified by preparative HPLC method A to give a solid (11.4 mg). MS (pos) m/z 263.1 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-a9c474a32c484e5b9c8603f8e9f62aea |
| Source note | uspto-grants-2010_02 |