HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 24809894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 5-(4-Nitrophenyl)-1,2-oxazole-4-carboxylic acid | HCID 22831707 | — |
| Product | HCID 24809894 | HCID 24809894 | — |
Reaction Steps
The title compound was prepared from 5-(4-nitrophenyl)isoxazole-4-carboxylic acid (11.7 mg, 0.050 mmol) and diethylamine (4.4 mg, 0.060 mmol) as described in synthetic method A and thereafter purified, first by preparative HPLC method A and then by method B, to give a solid (4.3 mg). MS (pos) m/z 290.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-cf6a9eedb47841c09209df0299ba7cc7 |
| Source note | uspto-grants-2010_02 |