HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 24809893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | 5-(4-methoxyphenyl)isoxazole-4-carboxylic acid | HCID 4997962 | — |
| Product | HCID 24809893 | HCID 24809893 | — |
Reaction Steps
The title compound was prepared from 5-(4-methoxyphenyl)isoxazole-4-carboxylic acid (11.0 mg, 0.050 mmol) and diethylamine (4.4 mg, 0.060 mmol) as described in synthetic method A and thereafter purified by preparative HPLC method A to give a solid (7.8 mg). MS (pos) m/z 275.2 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-8f7719f51ed94467ba33c9c77e26054e |
| Source note | uspto-grants-2010_02 |