HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 24809923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | 5-Phenylisoxazole-4-carboxylic acid | HCID 14787253 | — |
| Product | HCID 24809923 | HCID 24809923 | — |
Reaction Steps
The title compound was prepared from 5-(phenyl)isoxazole-4-carboxylic acid (9.5 mg, 0.050 mmol) and pyrrolidine (4.3 mg, 0.060 mmol) as described in synthetic method A and thereafter purified, first by preparative HPLC method A and then by method B, to give a solid (12.9 mg). MS (pos) m/z 243.2 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-4c7c64cd7b4b4cebb0c95c41be6364ce |
| Source note | uspto-grants-2010_02 |