HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisoamylamine → N,N-bis(3-Methylbutyl)-5-(4-methylphenyl)isoxazole-4-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisoamylamine | HCID 10988 | — |
| Reactant | 5-(p-Tolyl)isoxazole-4-carboxylic acid | HCID 22831706 | — |
| Product | N,N-bis(3-Methylbutyl)-5-(4-methylphenyl)isoxazole-4-carboxamide | HCID 24809988 | — |
Reaction Steps
The title compound was prepared from 5-(4-methylphenyl)isoxazole-4-carboxylic acid (10.2 mg, 0.050 mmol) and diisoamylamine (9.4 mg, 0.060 mmol) as described in synthetic method B and thereafter purified by preparative HPLC method B to give a solid (6.7 mg). Calcd for C21H30N2O2: 342.2307, found 342.2318.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-65be3168079b4b989590e792c965aca7 |
| Source note | uspto-grants-2010_02 |