HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic acid--3-(4-methoxyphenyl)pyrrolidine (1/1) → HCID 24809509, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic acid--3-(4-methoxyphenyl)pyrrolidine (1/1) | HCID 17749747 | — |
| Reactant | 5-(p-Tolyl)isoxazole-4-carboxylic acid | HCID 22831706 | — |
| Product | HCID 24809509 | HCID 24809509 | — |
Reaction Steps
The title compound was prepared from 5-(4-methylphenyl)isoxazole-4-carboxylic acid (10.2 mg, 0.050 mmol) and 3-(4-methoxyphenyl)pyrrolidine oxalat (16.0 mg, 0.060 mmol) as described in synthetic method B and thereafter purified by preparative HPLC method B to give a solid (4.3 mg). Calcd for C22H22N2O3: 362.1630, found 362.1636.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-a4eac07f6d054ea198491677ae610957 |
| Source note | uspto-grants-2010_02 |