HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic acid--3-(4-methoxyphenyl)pyrrolidine (1/1) → HCID 59170227, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic acid--3-(4-methoxyphenyl)pyrrolidine (1/1) | HCID 17749747 | — |
| Reactant | 4-Isoxazolecarboxylic acid, 5-[4-(trifluoromethyl)phenyl]- | HCID 68682921 | — |
| Product | HCID 59170227 | HCID 59170227 | — |
Reaction Steps
The title compound was prepared from 5-(4-trifluoromethylphenyl)isoxazole-4-carboxylic acid (12.9 mg, 0.050 mmol) and 3-(4-methoxyphenyl)pyrrolidine oxalat (16.0 mg, 0.060 mmol) as described in synthetic method C and thereafter purified by preparative HPLC method B to give a solid (6.5 mg). Calcd for C22H19F3N2O3: 416.1348, found 416.1348.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-8aab4b07a7ec4c4aaa4f303b0f326fd9 |
| Source note | uspto-grants-2010_02 |