HuagongsheHuagongshe Chemistry Print Report · For research reference only
1003561-85-0 → HCID 59170241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1003561-85-0 | HCID 17749814 | — |
| Reactant | 4-Isoxazolecarboxylic acid, 5-[4-(trifluoromethyl)phenyl]- | HCID 68682921 | — |
| Product | HCID 59170241 | HCID 59170241 | — |
Reaction Steps
The title compound was prepared from 5-(4-trifluoromethylphenyl)isoxazole-4-carboxylic acid (12.9 mg, 0.050 mmol) and 2-pyridin-3-yl thiomorpholine hydrochloride (13.0 mg, 0.060 mmol) as described in synthetic method C and thereafter purified by preparative HPLC method B to give a solid (12.8 mg). Calcd for C20H16F3N3O2S: 419.0915, found 419.0914.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07666888B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-fcaa74faefe843f1a05125b4d09d37b4 |
| Source note | uspto-grants-2010_02 |