Hydrochloric Acid → HCID 68542065, compound

Participants

Reaction Steps

Dissolve {4-[7-(2-diethylaminomethyl-pyridin-4-yl)-imidazo[1,2-a]pyridin-3-yl]-benzyl}-carbamic acid tert-butyl ester (0.24 g, 0.49 mmol) in dioxane (10 mL) under nitrogen. Add 4 M HCl in dioxane (5 mL) to the reaction and stir for 2 hours. Concentrate to dryness and use crude as the tri-HCl salt (0.321 g, crude). MS (ES), m/z 386.2 (M+1).

Provenance & Evidence