Diethylamine → HCID 20553473, compound

HRID 1446912Notes

Reaction equation

[ClH:1].[Cl:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[C:19]([CH:20]=1)=[N:18][C:17]1[C:12](=[CH:13][CH:14]=[C:15]([O:21][CH2:22][CH2:23][CH2:24]Cl)[CH:16]=1)[CH:11]=2.[CH2:26]([NH:28][CH2:29][CH3:30])[CH3:27]>>[ClH:2].[ClH:1].[ClH:2].[CH2:26]([N:28]([CH2:29][CH3:30])[CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[C:19]([CH:20]=1)=[N:18][C:17]1[C:12](=[CH:13][CH:14]=[C:15]([O:21][CH2:22][CH2:23][CH2:24][N:18]([CH2:19][CH3:10])[CH2:17][CH3:16])[CH:16]=1)[CH:11]=2)[CH3:27]

Participants

Reactant 2

HCID 8021Diethylamine

HCID 201846633,6-Bis(3-chloropropoxy)acridine--hydrogen chloride (1/1)

Product 1

HCID 20553473HCID 20553473, compound

Conditions

Temperature: 100 °C

Procedure

The compound is prepared from 3,6-bis(3-chloropropoxy)acridine hydrochloride and diethylamine as described in Example 15 except that the mixture is heated at 100° C. for 24 hours, giving 1.5 g. of the desired product as yellow crystals, m.p. 235°-236° C.

Workup

customgiving 1.5 g

Sources & evidence

ORD record: ord-f0239d3730a946e68610ca427fa9fa5c
Source dataset: uspto-grants-1982_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04314061

Reaction notes

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