HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-1,2,4-Triazole → 1-(3-Phenylpropyl)-1H-1,2,4-triazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (3-Bromopropyl)benzene | HCID 12503 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-(3-Phenylpropyl)-1H-1,2,4-triazole | HCID 20528532 | — |
Reaction Steps
A mixture of 14 parts by weight of 1,2,4-triazole, 200 parts by weight of acetonitrile, 32 parts by weight of potassium carbonate and 40 parts by weight of 3-phenylpropyl bromide is stirred for 12 hours. The mixture is then filtered and the filtrate is concentrated. Distillation gives 25 parts by weight of pure 1-(3-phenylpropyl)-1,2,4-triazole; b.p. (0.013 mbar): 114°-116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04315017 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-a8d69479e1bd405b8b207b23899cc8de |
| Source note | uspto-grants-1982_02 |