HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 20495221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Isobutyraldehyde | HCID 6561 | — |
| Reactant | 1H-1,2,4-Triazole | HCID 9257 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 20495221 | HCID 20495221 | — |
Reaction Steps
The diethylacetal of iso-butyraldehyde (2.8 g) was reacted with acetyl chloride (2.7 g) in the presence of copper bronze; the product was reacted with 1,2,4-triazole (3.0 g) in acetonitrile (50 ml) to give the title compound as a viscous oil which GLC showed to be slightly impure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04315016 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-3e304f77bc3e4003babf148aa728ffd0 |
| Source note | uspto-grants-1982_02 |