Benzaldehyde → HCID 20495230, compound

HRID 1447019Notes

Reaction equation

HRID 1447019 reaction equation
[CH:1](=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:9](Cl)(=O)[CH3:10].[NH:13]1[CH:17]=[N:16][CH:15]=[N:14]1>[Cu]>[N:13]1([C:3]2[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=2[CH2:1][O:8][CH2:9][CH3:10])[CH:17]=[N:16][CH:15]=[N:14]1

Participants

5

Reactant 3

HCID 240BenzaldehydeHCID 6367Acetyl chlorideHCID 92571H-1,2,4-Triazole

Product 1

HCID 20495230HCID 20495230, compound

Reagents, catalysts & solvents 1

HCID 23978CopperCatalyst

Procedure

The diethyl acetal of benzaldehyde (3.6 g) and acetyl chloride (2.5 g) were reacted in the presence of a trace of copper bronze. The product was reacted with 1,2,4-triazole (2.8 g) to give the title compound as a viscous oil which GLC showed to be about 95% pure.

Sources & evidence

ORD record
ord-67d1dbd9e772418dad71843e29e13fd3
Source dataset
uspto-grants-1982_02
Patent number
US04315016

Reaction notes

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