Acetyl chloride → HCID 57072213, compound

HRID 1447020Notes

Reaction equation

HRID 1447020 reaction equation
[Cl:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][CH:3]=1.[C:10](Cl)(=O)[CH3:11].[NH:14]1[CH:18]=[N:17][CH:16]=[N:15]1>[Cu]>[N:14]1([CH:6]([O:7][CH2:10][CH3:11])[C:5]2[CH:8]=[CH:9][C:2]([Cl:1])=[CH:3][CH:4]=2)[CH:18]=[N:17][CH:16]=[N:15]1

Participants

5

Reactant 3

HCID 6367Acetyl chlorideHCID 77264-ChlorobenzaldehydeHCID 92571H-1,2,4-Triazole

Product 1

HCID 57072213HCID 57072213, compound

Reagents, catalysts & solvents 1

HCID 23978CopperCatalyst

Procedure

The diethyl acetal of p-chlorobenzaldehyde (4.28 g) was reacted with acetyl chloride (2.34 g) in the presence of a trace of copper bronze. The product was reacted with 1,2,4-triazole (2.8 g) to give the title compound as a viscous oil.

Sources & evidence

ORD record
ord-16ab039f3e854b6e973614688c1abcde
Source dataset
uspto-grants-1982_02
Patent number
US04315016

Reaction notes

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