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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1447137Generated: November 1, 2026

Potassium Carbonate → HCID 12895163, compound

https://huagongshe.com/reaction/1447137

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantEpibromohydrinHCID 18430—
ReactantHCID 586077HCID 586077—
SolventDimethylformamideHCID 6228—
ProductHCID 12895163HCID 1289516393.8%

Reaction Conditions

Temperature50 °C

Reaction Steps

Using the method described in Example V, 35 g of 2-carboethoxy-3-hydroxy-4-butyl-5-methyl-pyrrole, 32 g of epibromohydrin and 41 g of dry potassium carbonate in 100 ml of N,N-dimethylformamide, when heated at 50° C. for 8 hours, give 41 g of 1-(2-carboethoxy-4-butyl-5-methyl-pyrrol-3-oxy)-2,3-epoxypropane, of melting point 125°-127° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04315939
Source datasetuspto-grants-1982_02
ORD IDord-d4f55c6c373d40bb9d4df60cbca273f0
Source noteuspto-grants-1982_02