HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 12801552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Epibromohydrin | HCID 18430 | — |
| Reactant | HCID 54730665 | HCID 54730665 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Product | HCID 12801552 | HCID 12801552 | 61.7% |
Reaction Steps
Using the method described in Example V, 20 g of 2-carboethoxy-3-hydroxy-4-benzyl-5-methyl-pyrrole, 14 g of epibromohydrin and 20 g of dry potassium carbonate in 150 ml of methyl isobutyl ketone give 15 g of 1-(2-carboethoxy-4-benzyl-5-methyl-pyrrol-3-oxy)-2,3-epoxypropane as a pale yellow, very viscous oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04315939 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-dbd4a4d333f442978fa3c5e54439a5fc |
| Source note | uspto-grants-1982_02 |