HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-enoyl chloride → HCID 57198396, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-enoyl chloride | HCID 66023 | — |
| Reactant | HCID 135503117 | HCID 135503117 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 57198396 | HCID 57198396 | 75% |
Reaction Steps
A mixture of 4.0 g (0.023 mole) of 4,5-dihydro-s-triazolo[3,4-c]benzo-as-triazine, 7.66 g (0.046 mole) of cinnamoyl chloride and 70 ml of dimethyl formamide is refluxed for 4 hours, and the mixture is processed in the usual way. 7.48 g (75%) of the title compound are obtained; m.p.: 220°-221° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04316022 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-1995b30f04a949829db8a5dc97f8efee |
| Source note | uspto-grants-1982_02 |