Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Stearoyl chloride | HCID 8212 | — |
| Reactant | HCID 135503117 | HCID 135503117 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13156318 | HCID 13156318 | 45% |
Reaction Steps
A mixture of 5 g (0.029 mole) of 4,5-dihydro-s-triazolo[3,4-c]benzo-as-triazine, 2 g (0.066 mole) of stearoyl chloride and 50 ml of dry dimethyl formamide is heated at 60° C. for one hour under argon atmosphere. The reaction mixture is poured onto ice and the product is filtered off. 8 g (45%) of the title compound are obtained; m.p.: 77°-78° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04316022 |
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| Source dataset | uspto-grants-1982_02 |
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| ORD ID | ord-c517e905ddca4215a7e125d5420d5cb7 |
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| Source note | uspto-grants-1982_02 |
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