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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1447169Generated: November 2, 2026

Stearoyl chloride → HCID 13156318, compound

https://huagongshe.com/reaction/1447169

Reaction equation

Participants

RoleNameHCIDCharge
ReactantStearoyl chlorideHCID 8212—
ReactantHCID 135503117HCID 135503117—
SolventDimethylformamideHCID 6228—
ProductHCID 13156318HCID 1315631845%

Reaction Conditions

Temperature60 °C

Reaction Steps

A mixture of 5 g (0.029 mole) of 4,5-dihydro-s-triazolo[3,4-c]benzo-as-triazine, 2 g (0.066 mole) of stearoyl chloride and 50 ml of dry dimethyl formamide is heated at 60° C. for one hour under argon atmosphere. The reaction mixture is poured onto ice and the product is filtered off. 8 g (45%) of the title compound are obtained; m.p.: 77°-78° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04316022
Source datasetuspto-grants-1982_02
ORD IDord-c517e905ddca4215a7e125d5420d5cb7
Source noteuspto-grants-1982_02