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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1447189Generated: November 3, 2026

Carbon Disulfide → 1-(2-Methoxyethyl)-4-phenylimidazolidine-2-thione

https://huagongshe.com/reaction/1447189

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCarbon DisulfideHCID 6348—
ReactantHCID 13035411HCID 13035411—
SolventO-XyleneHCID 7237—
Product1-(2-Methoxyethyl)-4-phenylimidazolidine-2-thioneHCID 12803437—

Reaction Conditions

Temperature130 °C

Reaction Steps

The ethylamine product of Example IV in the amount of 6.85 g is dissolved in 20 ml xylene, and this is then stirred with 3 ml carbon disulfide at room temperature for two hours. The resulting slurry is then slowly heated to 130° C. and maintained at this temperature for four hours.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04316038
Source datasetuspto-grants-1982_02
ORD IDord-42c6909872844086ab5e65c7137809a4
Source noteuspto-grants-1982_02