Carbon Disulfide → 1-(2-Methoxyethyl)-4-phenylimidazolidine-2-thione
Reaction equation
[NH2:1][CH:2]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)[CH2:3][NH:4][CH2:5][CH2:6][O:7][CH3:8].[C:15](=S)=[S:16]>C1(C)C(C)=CC=CC=1>[CH3:8][O:7][CH2:6][CH2:5][N:4]1[CH2:3][CH:2]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)[NH:1][C:15]1=[S:16]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 130 °C
Procedure
The ethylamine product of Example IV in the amount of 6.85 g is dissolved in 20 ml xylene, and this is then stirred with 3 ml carbon disulfide at room temperature for two hours. The resulting slurry is then slowly heated to 130° C. and maintained at this temperature for four hours.
Workup
- temperaturemaintained at this temperature for four hours
Sources & evidence
- ORD record
- ord-42c6909872844086ab5e65c7137809a4
- Source dataset
- uspto-grants-1982_02
- Patent number
- US04316038
Reaction notes
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