HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13205870, compound → HCID 13205871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13205870 | HCID 13205870 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 13205871 | HCID 13205871 | — |
Reaction Steps
20 g 2-(N-isopropyl-N-carbomethoxyamino)-4-methyl-4'-fluoro-2,5-dihydrobenzophenone and 100 g manganese dioxide in 200 ml chloroform are stirred 4 hours under reflux. The reaction mixture is cooled, filtered and evaporated in vacuo. The residue is recrystallised from hexane to obtain the heading compound, m.p. 92°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04316042 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-829053cd9ef64de6941a40012ebb61a0 |
| Source note | uspto-grants-1982_02 |