HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 20550608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Reactant | 2-Methyl-4,6-dinitroaniline | HCID 345304 | — |
| Reactant | HCID 22318895 | HCID 22318895 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20550608 | HCID 20550608 | — |
Reaction Steps
40 of 6-methyl-2,4-dinitroaniline are stirred for 4 hours at 80° C. in 500 parts of toluene with 34 parts of chlorosulfonyl isocyanate. The suspension of the chlorosulfonyl urea obtained is mixed at 25° C. with 40 parts of water and saponified at 60° C. to give 6-methyl-2,4-dinitrophenyl urea.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04316861 |
| Source dataset | uspto-grants-1982_02 |
| ORD ID | ord-d44cbd0ccdae403dbcb1b2c68cd068ff |
| Source note | uspto-grants-1982_02 |