HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 70609554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | HCID 70609867 | HCID 70609867 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 70609554 | HCID 70609554 | 95.9% |
Reaction Steps
The bromide from Example XIX (7.5 g, 0.024 mol) was dissolved in butan-2-one (70 ml), after which powdered potassium iodide (6.8 g, 0.04 mol) and pyridine (0.2 ml) were added. The mixture was refluxed for 11/2 hours, mixed with ether, and filtered. Evaporation yielded 8.2 g product (95% by weight yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04177197 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-f7a582e15ccb40bd9c45a932165446f4 |
| Source note | uspto-grants-1979_12 |