HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexyl isocyanate → HCID 12608488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexyl isocyanate | HCID 18502 | — |
| Reactant | 3-[2-(4-Aminopiperidyl)ethyl]indole, hydrate | HCID 20384353 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12608488 | HCID 12608488 | 102.7% |
Reaction Steps
4-Amino-1-[2-(3-indolyl)ethyl]piperidine, hydrate (1.307 g, 0.005 mole) in benzene (50 ml.) was treated with cyclohexyl isocyanate (0.688 g, 0.0055 mole) and the mixture stirred for 18 hrs. Filtration afforded the title compound as colourless prisms (1.893 g), m.p. 203.8°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04177279 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-ecd7cce690254d44bf65acacb1f8d43b |
| Source note | uspto-grants-1979_12 |