HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 53865071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 2-Morpholinoethylamine | HCID 408285 | — |
| Reactant | HCID 20384409 | HCID 20384409 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53865071 | HCID 53865071 | — |
Reaction Steps
A solution of 13 g (0.05 mol) of N,N-diphenylcarbamoylacetic acid and 7.1 g (0.055 mol) of N-(2-aminoethyl)morpholine in 120 ml of methylene chloride is refluxed with agitation. A solution of 11 g (0.055 mol) of dicyclohexylcarbodiimide in 30 ml of CH2Cl2 is slowly added and the mixture is maintained under reflux for 3 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04177290 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-ea69a5ed8a12469c845113ba8e3e56a7 |
| Source note | uspto-grants-1979_12 |