Indacrinone → 76698-88-9

HRID 1447702Notes

Reaction equation

HRID 1447702 reaction equation
[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([OH:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][C:3]1([CH3:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.C(=O)(O)[O-].[Na+:29]>O>[O:1]=[C:2]1[C:10]2[C:5](=[CH:6][C:7]([O:13][CH2:14][C:15]([O-:17])=[O:16])=[C:8]([Cl:12])[C:9]=2[Cl:11])[CH2:4][C:3]1([CH3:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.[Na+:29]

Participants

4

Reactant 2

HCID 42266IndacrinoneHCID 516892Sodium Bicarbonate

Product 1

HCID 8673578076698-88-9

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

(1-Oxo-2-methyl-2-phenyl-6,7-dichloro-5-indanyloxy)acetic acid (1 gm.) is treated with sodium bicarbonate (0.25 gm.) in water (10 ml.) and the mixture stirred and heated to effect solution. The solution is diluted with water to a volume of 50 ml. and sterilized by autoclaving at 120° C. for one hour.

Workup

  1. temperatureheated

Sources & evidence

ORD record
ord-223304b09c804f1cbc37c3c3342272d4
Source dataset
uspto-grants-1979_12
Patent number
US04177285

Reaction notes

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