Ethanol → HCID 20382544, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 11.7 parts of 3-mercapto-5-(4-tert.-butylphenyl)-1,2,4-triazole, 12.5 parts of 1-bromododecane and 100 parts by volume of ethyl alcohol was heated at reflux temperature for four hours. After cooling to 20° C., a four percent weight/volume aqueous sodium hydroxide solution was added followed by 100 parts by volume of water. The precipitated product was filtered and dried yielding 59 percent of 3-(n-dodecylthio)-5-(4-tert.butylphenyl)-1,2,4-triazole which had a melting point of 87°-92° and the following elemental analysis:

Provenance & Evidence