HRID1447787

反应详情

EQUATION

反应方程式

HRID 1447787 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 5 g of 2A and 5.7 g of 2-propenamine in 50 ml of ethanol was refluxed for 6 days. Stripping of the solvent, followed by charcoal treatment of the product and recrystallization of the treated product from ether-hexane, gave 2, as white crystals, mp: 114.5°-115.5° C.

WORKUP

后处理

  1. customStripping of the solvent, followed by charcoal treatment of the product and recrystallization of the treated product from ether-hexane
  2. customgave 2