Hydrazine hydrate (1:1) → HCID 85945302, compound

HRID 1447812Notes

Reaction equation

HRID 1447812 reaction equation
[C:1]([O:15]CC)(=O)[CH2:2][O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][CH2:10][CH2:11][O:12][CH3:13].O.[NH2:19][NH2:20]>C(O)C>[C:1]([NH:19][NH2:20])(=[O:15])[CH2:2][O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][CH2:10][CH2:11][O:12][CH3:13]

Participants

4

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 20383039HCID 20383039, compound

Product 1

HCID 85945302HCID 85945302, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A solution of 61 g (0.244 mol) of crude ethyl 3,6,9,12-tetra-oxa-tridecanoate and 25 ml (0.488 mol) of hydrazine hydrate in 600 ml of ethanol is left to stand for 25 hours at 25°. The reaction mixture is evaporated and the crude, oily 3,6,9,12-tetra-oxa-tridecanoic acid hydrazide, which is thus obtained, is further processed direct.

Workup

  1. customThe reaction mixture is evaporated

Sources & evidence

ORD record
ord-d39b75c57cd04e45b3de201aee460aae
Source dataset
uspto-grants-1979_12
Patent number
US04178378

Reaction notes

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