HRID1448016

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID4873

Potassium chloride

ClK

HCID5234

Sodium chloride

ClNa

HCID433294

Lithium Chloride

ClLi

结构：CC(C)C(=O)CC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3C[C@H](O)[C@@H]4C[C@H](O)CC[C@]4(C)[C@H]3CC[C@]12C.CS(=O)(=O)O.CS(=O)(=O)O

HCID86736736

未命名化合物

PRODUCTS

生成物

结构：CC(C)C(=O)CC[C@@H](C)[C@H]1CC[C@H]2[C@@H]3CC=C4CC(Cl)CC[C@]4(C)[C@H]3CC[C@]12C

HCID54230696

未命名化合物

PROCEDURE

实验过程

3α,6α-Dihydroxy-5β-cholestan-24-one (I) is mesylated in a conventional manner to form 3α,6α-dihydroxy-5β-cholestan-24-one dimesylate (VI). Then the compound (VI) is reacted with an inorganic salt such as potassium chloride, sodium chloride or lithium chloride to give 3-chlorocholest-5-en-24-one (VII).