HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Chloride → 3-Chlorocholest-5-en-24-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Chloride | HCID 4873 | — |
| Reactant | Sodium Chloride | HCID 5234 | — |
| Reactant | Lithium Chloride | HCID 433294 | — |
| Reactant | HCID 86736736 | HCID 86736736 | — |
| Product | 3-Chlorocholest-5-en-24-one | HCID 54230696 | — |
Reaction Steps
3α,6α-Dihydroxy-5β-cholestan-24-one (I) is mesylated in a conventional manner to form 3α,6α-dihydroxy-5β-cholestan-24-one dimesylate (VI). Then the compound (VI) is reacted with an inorganic salt such as potassium chloride, sodium chloride or lithium chloride to give 3-chlorocholest-5-en-24-one (VII).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04179452 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-93132d3387db405083bb408e43e6a48b |
| Source note | uspto-grants-1979_12 |