HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 54017040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 54533821 | HCID 54533821 | — |
| Reactant | HCID 86736740 | HCID 86736740 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 54017040 | HCID 54017040 | 7.8% |
Reaction Steps
Prepared as in Example 1 by reacting 2.78 g (0.021 m) of 2-nitro-2-methylpropionaldoxime, 5.0 g (0.21 m) of N-methyl-N-(2,4-dimethyl-3-oxo-2-pentanesulfenyl)carbamoyl fluoride and 2.13 g (0.021 m) of triethylamine in 50 ml of dioxane. The product was purified by column chromatography to yield 0.55 g of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04179514 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-be442cbe398b4a09bd8b9f6bc50d3a81 |
| Source note | uspto-grants-1979_12 |