Triethylamine → HCID 54328425, compound

Participants

Reaction Steps

To a solution of 2.5 g (0.015 m) of 3,5,5-trimethyl-2-oximino-thiazolidin-4-one and 3.93 g (0.015 m) of N-methyl-N-(2-benzoyl-2-propanesulfenyl)carbamoyl chloride in 100 ml of dioxane was added 1.5 g (0.015 m) of triethylamine. After stirring at room temperature for 16 hours, the reaction mixture was diluted with water and the product isolated in ethylacetate. Recrystallized from isopropyl ether. Weight of the procut 1.3 g, m.p. 98°-100° C.

Provenance & Evidence