HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20298835, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Methyl-1-propyl-1,3-benzodiazole-5-carboxylic acid | HCID 20298856 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20298835 | HCID 20298835 | — |
Reaction Steps
To a stirred mixture of 18 parts of 2-methyl-1-propyl-1H-benzimidazole-5-carboxylic acid and 150 parts of trichloromethane are added dropwise 29.8 parts of thionyl chloride. Upon completion, stirring is continued for 20 minutes at reflux. The reaction mixture is cooled, dried, filtered and evaporated, yielding 22.5 parts of 2-methyl-1-propyl-1H-benzimidazole-5-carbonyl chloride monohydrochloride as a residue.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04179505 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-a778eae569254d1cabce940752985c51 |
| Source note | uspto-grants-1979_12 |