Dichloromethane → HCID 70606969, compound

Participants

Reaction Steps

To a solution of 12 g of 3-phenoxy-5-piperazinylpyridine N-oxide and 0.5 g of dichloromethane in 100 ml of ethanol is added 1 g of 20% Palladium on charcoal. The suspension is shaken under a pressure of 50 pounds per square inch of hydrogen atmosphere until no further drop in pressure occurs. The solution is filtered and concentrated in vacuo to give 3-phenoxy-5-piperazinylpyridine monohydrochloride; mp 191°-192.5° C. dec.

Provenance & Evidence