3,4-Dichloroaniline → HCID 20376419, compound

HRID 1448453Notes

Reaction equation

HRID 1448453 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[Cl:9])[NH2:5].Cl.Cl[CH2:12][CH2:13][N:14]([CH3:16])[CH3:15].C(=O)(O)[O-].[Na+]>>[CH3:15][N:14]([CH3:16])[CH2:13][CH2:12][NH:5][C:4]1[CH:6]=[CH:7][C:8]([Cl:9])=[C:2]([Cl:1])[CH:3]=1

Participants

4

Reactant 3

HCID 72573,4-DichloroanilineHCID 516892Sodium BicarbonateHCID 11636816N,N-Dimethylaminoethyl chloride hydrochloride

Product 1

HCID 20376419HCID 20376419, compound

Procedure

In the manner given in Example 1, 3,4-dichloroaniline, 1-chloro-2-dimethylaminoethane hydrochloride, and sodium bicarbonate are heated to give N,N-dimethyl-N'-(3,4-dichlorophenyl)ethylenediamine.

Workup

  1. temperatureare heated

Sources & evidence

ORD record
ord-afb9eacfe8564c4fafbd9af4576ae3b4
Source dataset
uspto-grants-1979_12
Patent number
US04180522

Reaction notes

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