Magnesium Hydroxide → HCID 22027098, compound

HRID 1448505Notes

Reaction equation

HRID 1448505 reaction equation
[OH-].[Mg+2:2].[OH-].[C:4]([O-:15])(=[O:14])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([CH3:13])([CH3:12])[CH3:11]>O>[C:4]([O-:15])(=[O:14])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([CH3:11])([CH3:12])[CH3:13].[Mg+2:2].[C:4]([O-:15])(=[O:14])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]([CH3:11])([CH3:12])[CH3:13]

Participants

4

Reactant 2

HCID 73981Magnesium HydroxideHCID 21225528Neodecanoate

Product 1

HCID 22027098HCID 22027098, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Conditions

Temperature
95 °C

Procedure

A solution of magnesium neo decanoate was prepared by adding 1.07 lbs. of magnesium hydroxide and 5.23 lbs. of neo decanoate acid to 380 lbs. of water in a stainless steel drum fitted with an agitator and a metal coil for heating and cooling. The mixture was heated to 95° C. for three hours with good agitation then cooled to 25° C. Water was added to make up for that lost by evaporation, and 0.1 lb. (0.025%) of Triton X-305 was added. The mixture was filtered through fluted filter paper. The solution contained 780 ppm magnesium or 1.18% by weight of magnesium neo decanoate.

Workup

  1. additionby adding 1.07 lbs
  2. temperaturea metal coil for heating
  3. temperaturecooling
  4. temperaturethen cooled to 25° C
  5. customthat lost by evaporation, and 0.1 lb
  6. addition(0.025%) of Triton X-305 was added
  7. filtrationThe mixture was filtered
  8. filtrationthrough fluted filter paper

Sources & evidence

ORD record
ord-37d730aac3a14fa191013fd63a21fa9d
Source dataset
uspto-grants-1979_12
Patent number
US04180620

Reaction notes

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