HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20380297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Olivetol | HCID 10377 | — |
| Reactant | 1-Methyl-4-piperidone | HCID 74049 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20380297 | HCID 20380297 | 79% |
Reaction Steps
Olivetol (22.3 g) and N-methyl-4 -piperidone (14 g) were dissolved in 50 ml acetic acid and treated with HCl gas as described in Example VI giving 30.6 g (79%) product, m.p. 179°-180°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04180669 |
| Source dataset | uspto-grants-1979_12 |
| ORD ID | ord-d040a3be0e594d5b8bdb07288ab11c6c |
| Source note | uspto-grants-1979_12 |