Hydrochloric Acid → HCID 54411758, compound

HRID 1448593Notes

Reaction equation

HRID 1448593 reaction equation
O.[C:2]1([OH:10])[CH:9]=[C:7]([CH3:8])[CH:6]=[C:4]([OH:5])[CH:3]=1.[CH3:11][N:12]1[CH2:17][CH2:16][CH2:15][CH2:14][C:13]1=O.Cl>C(O)(=O)C>[CH3:11][N:12]1[CH:13]=[CH:14][CH:15]([C:3]2[C:2]([OH:10])=[CH:9][C:7]([CH3:8])=[CH:6][C:4]=2[OH:5])[CH2:16][CH2:17]1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 13603N-Methyl-2-piperidoneHCID 3083941Resorcinol, 5-methyl-, monohydrate

Product 1

HCID 54411758HCID 54411758, compoundYield 30.1%

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Orcinol hydrate (15 g) and N-methylpiperidone (11.0 g) were dissolved in 30 ml acetic acid and treated with HCl gas as described in Example VI giving 6.42 g of product, m.p. 241°-243°.

Sources & evidence

ORD record
ord-53ea2b7c038245d383fb5bd7734c5052
Source dataset
uspto-grants-1979_12
Patent number
US04180669

Reaction notes

Loading…