Hydrochloric Acid → HCID 20380305, compound

HRID 1448594Notes

Reaction equation

HRID 1448594 reaction equation
[CH:1]([C:4]1[CH:5]=[C:6]([OH:11])[CH:7]=[C:8]([CH:10]=1)[OH:9])([CH3:3])[CH3:2].[CH2:12]([N:19]1[CH2:24][CH2:23][C:22](=O)[CH2:21][CH2:20]1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[ClH:26]>C(O)(=O)C>[ClH:26].[CH2:12]([N:19]1[CH2:20][CH:21]=[C:22]([C:7]2[C:8]([OH:9])=[CH:10][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:5][C:6]=2[OH:11])[CH2:23][CH2:24]1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 192201-Benzyl-4-piperidoneHCID 127958995-(Propan-2-yl)benzene-1,3-diol

Product 1

HCID 20380305HCID 20380305, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

5-Isopropyl resorcinol (20.2 g), N-benzyl-4-piperidone (24.6 g) and 45 ml acetic acid was treated with HCl gas as described in Example VI to give 39.15 g product, m.p. 286°-288°.

Sources & evidence

ORD record
ord-2a8c307de68349419e11dc9a5de5c447
Source dataset
uspto-grants-1979_12
Patent number
US04180669

Reaction notes

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