Hydrazine hydrate (1:1) → HCID 54103907, compound

HRID 1448702Notes

Reaction equation

HRID 1448702 reaction equation
[N+](C1C=CC(C[O:9][C:10](=[O:49])[C@H:11]([CH2:42][C:43]2[CH:48]=[CH:47][CH:46]=[CH:45][CH:44]=2)[NH:12][C:13](=[O:41])[C@@H:14]2[CH2:18][CH2:17][CH2:16][N:15]2[C:19](=[O:40])[CH2:20][NH:21][C:22](=[O:39])[C@H:23]([CH2:32][C:33]2[CH:38]=[CH:37][CH:36]=[CH:35][CH:34]=2)[NH:24][C:25]([O:27][C:28]([CH3:31])([CH3:30])[CH3:29])=[O:26])=CC=1)([O-])=O.O.NN>>[C:28]([O:27][C:25]([NH:24][C@H:23]([C:22]([NH:21][CH2:20][C:19]([N:15]1[CH2:16][CH2:17][CH2:18][C@H:14]1[C:13]([NH:12][C@H:11]([C:10]([OH:49])=[O:9])[CH2:42][C:43]1[CH:44]=[CH:45][CH:46]=[CH:47][CH:48]=1)=[O:41])=[O:40])=[O:39])[CH2:32][C:33]1[CH:34]=[CH:35][CH:36]=[CH:37][CH:38]=1)=[O:26])([CH3:31])([CH3:29])[CH3:30]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 13644462HCID 13644462, compound

Product 1

HCID 54103907HCID 54103907, compound

Procedure

the product of stage (g) is treated with hydrazine hydrate to obtain hydrazide of tert-butoxycarbonylphenylalanylglycylprolylphenylalanine;

Sources & evidence

ORD record
ord-8f32f62688db45fd8c010f6115e14c80
Source dataset
uspto-grants-1980_02
Patent number
US04187217

Reaction notes

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