Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chromic Acid | HCID 24425 | — |
| Reactant | HCID 53882190 | HCID 53882190 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 12734622 | HCID 12734622 | — |
Reaction Steps
A solution of 13.2 g. (0.0928 moles) cis/trans-1-(2-methylcyclohexyl)-1-ethanol in 50 ml. of ether was chilled in an ice bath and 50 ml. 2 N chromic acid solution (BROWN GARG-Reagent) was added dropwise, with stirring, at such a rate as to maintain the temperature at about 10° C. After the addition was complete, the ice bath was removed and the stirring was continued at ambient temperature for one hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04187251 |
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| Source dataset | uspto-grants-1980_02 |
|---|
| ORD ID | ord-2f6972e9508545dca6311ef789d0fcd5 |
|---|
| Source note | uspto-grants-1980_02 |
|---|
